Team:UCLA/Notebook/Materials/14 May 2015

  • Degummed more silk (2.5 grams)
  • pipetted 100 uL of the dialyzed silk from Tuesday to determine concentration
  • Spun more cellulose acetate (same conditions from yesterday)
  • prepared LiBr solution (16 mL, 9.3M)
  • took light microscope images of the fibers obtained yesterday
  • cellulose acetate fiber 20% at 20x mag
    • The spun fiber is approximately the same diameter as the PEEK tubing. For reference, the inner diameter of the PEEK tubing is 127 um.
    cellulose acetate fiber 20% at 20x mag
    • However, note that the fiber is non-uniform. This is an image of a different spot along the same fiber. This part of the fiber is likely thicker because the dope bent while coagulating in the bath.