Team:UCLA/Notebook/Spider Silk Genetics/30 July 2015
Contents
7/30/2015
Transformation Results
- Colonies Present on M2-15(1C3) and M2-12(T7) plates.
- Plan to do pick 4 colonies and analyze via colony PCR.
ICA for M1-9
- 45 minute initiator incubation time.
- 100 uL washes.
- 4 min ligation time at RT.
- Prepared the reaction mixtures ahead of time.
- Elute in 0.01% Tween-20
- 95 C for 5 min.
PCR Amplification for M1-9
- 1x 50 uL reaction.
- Used ICA eluate as template, amplified using post-elution primers.
Volume (uL) | |
---|---|
5x Q5 buffer | 10 |
10 mM dNTPs | 1 |
10 uM For (F-03) | 2.5 |
10 uM Rev (G-03) | 2.5 |
Template | 1 |
Q5 Polymerase | 0.5 |
ddH2O | 32.5 |
Total | 50 |
98 C | 30 sec |
---|---|
98 C | 10 sec |
66 C | 20 sec |
72 C | 30 sec |
repeat from step 2 | 20x |
72 C | 2 min |
12 C | hold |
Colony PCR for M2-12(T7), M2-15(1C3)
- Picked 4 colonies from each. Resuspended in 50 uL LB. Used 1 uL of resuspended colony as template.
- used 2x Taq Red for colony PCR
- Total 12.5 uL reaction for each colony.
Volume (uL) | |
---|---|
2x Taq Red | 6.25 |
10 uM For (VF) | 0.625 |
10 uM Rev (VR) | 0.625 |
Colony | 1 |
ddH2O | 4 |
Total | 12.5 |
95 C | 3 min |
95 C | 25 sec |
56 C | 30 sec |
72 C | 1 min |
repeat from step 2 | 30x |
72 C | 5 min |
12 C | hold |
Results
- Cast 1% TAE gel. Used 2 uL of NEB 1 kb ladder.
- Visualized M1-9 and colony PCR results.
- The PCR amplification of M1-9 was successful. The band at 1018 kb was excised for gel purification.
- Colonies 1, 2, 3, 4 for M2-12(T7) all appear to be correct. Will choose 3 for liquid culture and sequencing.
- Colonies 1, 2 for M2-15(1C3) appear to be correct. Colonies 3, 4 appear incorrect. Will send colonies 1, 2 for sequencing, as well as one more picked colony from the plate.
Liquid Culture
- Prepared 3x 5 uL cultures for M2-12(T7) and M2-15(1C3) each.
- Inoculated with 25 uL of colony resuspended in 50 uL of LB.